FT-IR laboratory

I. FT-IR BRUKER VERTEX 70V VACUUM SPECTROMETER INTEGRATED WITH HYPERION 3000 FT-IR MICROSCOPE (Fig. 1)

    Parameters:

  • Spectral range: 8000 cm-1 – 10 cm-1
  • Excitation sources:
    • MIR – high-energy ceramic source
    • FIR – mercury lamp
  • Beamsplitters:
    • MIR (8000 cm-1 – 350 cm-1)
    • MIR-FIR (6000 cm-1 – 50 cm-1)
    • FIR1 (680 cm-1 – 30 cm-1)
    • FIR2 (55 cm-1 – 10 cm-1)
  • Detectors (Vertex 70v/Hyperion 3000):
    • DLATGS (KBr)
    • MIR-FIR (KBr)
    • DLATGS (PE)
    • MCT
    • FPA
    • Bolometer
  • Objectives: vis, 15x, 36x, 20x (ATR)
  • Additional attachments for measurements in the vacuum chamber Vertex 70v:
    • Transmission
    • ATR (diamond)
    • AutoSeagull


Fig. 1. FT-IR Bruker Vertex 70v vacuum spectrometer integrated with HYPERION 3000 FT-IR microscope.

II. FT-IR FAST IMAGING MICROSCOPE NICOLET IN10 MX INTEGRATED WITH IZ10 SPECTROMETER (Fig. 2)

    Parameters:

  • Excitation sources: high-energy ceramic source
  • Detectors:
    • DLATGS (KBr) (7600–450 cm-1)
    • MCT-A (7800–650 cm-1)
    • MCT-A linear array (7800–720 cm-1)
  • Accessories:
    • ATR germanium
    • ATR diamond
    • transmission
  • 15x magnification objective


Fig. 2. Thermo Scientific Nicolet iN10 MX FT-IR fast imaging microscope integrated with iZ10 spectrometer.

III. NICOLET IS5 FT-IR SPECTROMETER (Fig. 3)

    Parameters:

  • Spectral range: 7800 cm-1 – 350 cm-1
  • Excitation source: Mid-infrared Ever-Glo high-energy ceramic source
  • Temperature controlled solid-state near-IR diode laser
  • Detectors:
    • DLATGS (KBr)
  • Accessories:
    • ATR (ZnSe)
    • transmission


Fig. 3. Nicolet Thermo Scientific iS5 FT-IR spectrometer.